Anonymous

Equipment/High Vacuum Station: Difference between revisions

From London Hackspace Wiki
m
Updated information on diffusion pump specification and fluid options
m (Updated information on diffusion pump specification and fluid options)
Line 33: Line 33:
===Diffusion pump===
===Diffusion pump===


The diffusion pump, as well as the majority of the vacuum manifolds and high-vacuum parts are from James Collings. A diffusion pump operates from approximately 10-30mbar down to as low as 10^-10mbar, though we are unlikely to be able to reach that extreme. 10^-6mbar (0.000001mbar) seems likely though.
The diffusion pump donated by James Collings is an Edwards E04. It's ultimate vacuum capacity is 5x10^-7 mbar (0.0000005mbar) with a pumping speed of air of ISO 600l/s^-1 (hydrogen: ISO 800l/s^-1). It has a maximum starting pressure of 300 mbar and requires a backing pump capable of keeping the backing pressure at about 1mbar (assuming DC704EU pump fluid).
Recommended backing pumps are the Edwards RV8 or RV12. The RV8 has a displacement of 9.7m^3h^-1 and an ultimate pressure of 2x10^-3. The RV12 is advised for fast roughing, has a displacement of 14.2m^3/h^-1 and an ultimate pressure of 2x10^-3 mbar.


The diff pump operates by boiling a special silicone oil to vapour and forcing it out through special baffles onto a water-cooled jacket. There the oil re-condenses and trickles down along with any air molecules it grabbed on the way. It sets up a pressure differential across the pump, where at its exist it should be at a high enough pressure the backing pump will be able to pump it away.
The diff pump operates by boiling a special silicone oil to vapour and forcing it out through special baffles onto a water-cooled jacket. There the oil re-condenses and trickles down along with any air molecules it grabbed on the way. It sets up a pressure differential across the pump, where at its exist it should be at a high enough pressure the backing pump will be able to pump it away.


Currently the recommended pump fluid for the Edwards E04 is Santovac 5. This is currently priced at £220 per 100ml. The pump takes a maximum fluid load of 175ml. If the existing pump fluid is unable to be used, getting the pump running will cost £440 in fresh fluid.
Current prices for the compatible fluids (as of October 6th, 2011, direct from Edwards Vacuum) are;
Please remember this when discussing if we really need to be worried about contaminating the pump.
 
* DC702 fluid - £117, 500ml (critical backing pressure 1.3 mbar, ultimate pressure 5x10^-6 mbar)
* DC704EU fluid - £134.10, 500ml (critical backing pressure 1.0 mbar, ultimate pressure 5x10^-7 mbar)
* DC705 fluid - £211.50, 500ml (critical backing pressure 0.9 mbar, ultimate pressure 5x10^-7 mbar)
* Santovac 5 fluid - £852.30, 500ml (critical backing pressure 0.8 mbar, ultimate pressure 5x10^-7 mbar)
* Edwards L9 fluid - Unknown price, possibly discontinued (critical backing pressure 0.9 mbar, ultimate pressure 5x10^-7 mbar)
 
On this I would recommend DC704EU fluid. For £17 extra you can achieve a magnitude better vacuum than the absolute cheapest. The spec sheet also describes it as a good durable and general-purpose fluid.


====Cold baffle====
====Cold baffle====